| 引用本文: | 白琦,勝間田五郎,陈修身,白瑛,梅树常.HPLC测定茄尼醇的不确定度[J].中国现代应用药学,2009,(3):240-242. |
| BAI Qi1,KATSUMATA GOROH2,CHEN Xiushen2,BAI ying2,MEI Shuchang2.Uncertainty Measurement in the HPLC Determination of Solanesol[J].Chin J Mod Appl Pharm(中国现代应用药学),2009,(3):240-242. |
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| 摘要: |
| 目的使高纯度茄尼醇(90%以上)含量的测定准确及可靠。方法建立了HPLC测定高纯度茄尼醇的不确定度的评定方法。结果通过统计学方法,量化不确定度分量,计算合成不确定度和扩展不确定度。结论仪器环境不变时测量结果受控。 |
| 关键词: 高效液相色谱法 茄尼醇 不确定度 |
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| Uncertainty Measurement in the HPLC Determination of Solanesol |
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BAI Qi1,KATSUMATA GOROH2,CHEN Xiushen2,BAI ying2,MEI Shuchang2
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| Abstract: |
| OBJECTIVE To make the measures of the content of solanesol under control. METHODSTo establish a method for uncertainty analysis in HPLC determination. RESULTSAll the standard uncertainties were then divided according to the appropriate rules to give a combined standard uncertainty and an expanded standard uncertainty. CONCLUSIONMeasures result is controllable under constant instrument environment. |
| Key words: HPLC solanesol uncertainty |
