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引用本文:黎小伟,蒋受军,周天详,庞兴寿.壮药阴香皮药材质量标准研究[J].中国现代应用药学,2012,29(10):899-902.
LI Xiaowei,JIANG Shoujun,ZHOU Tianxiang,PANG Xingshou.Criteria of Quality Control for Burmann Cinnamon Bark[J].Chin J Mod Appl Pharm(中国现代应用药学),2012,29(10):899-902.
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壮药阴香皮药材质量标准研究
黎小伟, 蒋受军, 周天详, 庞兴寿
广西玉林食品药品检验所,广西 玉林 537000
摘要:
目的 制定壮药阴香皮药材质量标准,为阴香皮药用植物资源的开发利用提供实验依据。方法 对10批阴香皮药材进行药材性状、显微特征、薄层色谱方面的研究,并测定其挥发油含量、总灰分、水分,采用气相色谱法测定阴香皮活性成分龙脑的含量。结果 不同来源阴香皮药材性状、显微特征、薄层色谱鉴别特征明显且一致性好;龙脑在0.052 8~ 1.056 μg 内呈良好的线性关系(r=0.999 9),平均加样回收率98.8 %(RSD=1.0%)。结论 本实验为制定壮药阴香皮质量控制标准提供了实验依据。
关键词:  阴香皮  质量标准  龙脑  TLC  GC
DOI:
分类号:
基金项目:广西壮族自治区壮药质量标准(第二卷)研究项目(MZY2010066)
Criteria of Quality Control for Burmann Cinnamon Bark
LI Xiaowei, JIANG Shoujun, ZHOU Tianxiang, PANG Xingshou
Yulin Institute for Food and Drug Control, Yulin 537000, China
Abstract:
OBJECTIVE To provide experiment basis by setting up the quality control specification of Burmann Cinnamon Bark. METHODS The pharmacognostic methods were employed. The volatile oils, ash content and moisture were determined by gas chromatography. RESULTS The morphological and histological characters of Burmann Cinnamon Bark from different origins were observed, the results showed good consistency. There was a good linear relationship of borneol in the range of 0.052 8-1.056 μg(r=0.999 9), the average recovery was 98.8% (RSD=1.0%). CONCLUSION The method provides reference for the quality control of Burmann Cinnamon Bark.
Key words:  Burmann Cinnamon Bark  quality criteria  borneol  TLC  GC
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