杞菊地黄口服液中芍药甙的HPLC测定和山茱萸的HPLC鉴别

余洪

引用本文:	余洪.杞菊地黄口服液中芍药甙的HPLC测定和山茱萸的HPLC鉴别[J].中国现代应用药学,1994,(5):22-23.
	Yu Hong.Determination of Paeonitlorin and Identification of Fructus Corni inQijudihuang Koufuye by HPLC[J].Chin J Mod Appl Pharm(中国现代应用药学),1994,(5):22-23.

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杞菊地黄口服液中芍药甙的HPLC测定和山茱萸的HPLC鉴别
余洪

作者	单位
余洪

摘要:

应用高效波相色谱法测定杞菊地黄口服液中芍药甙的含量。样品用正丁醇提取,YWGC8柱,流动相为乙腈—水(13:87),峰面积定量。方法准确,重现性好,平均加样回收率为99.0%,CV为1.01%。以山茱萸为对照药材,能同时鉴别样品中的山茱萸。本法适用于该制剂的质量控制。

关键词: 杞菊地黄口服液芍药甙山茱萸含量测定鉴别 HPLC

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Determination of Paeonitlorin and Identification of Fructus Corni inQijudihuang Koufuye by HPLC

Yu Hong

Abstract:

The content of Paeoniflorin in Qijudihuang Koufuye was determined by HPLC.The sample was extracted with butyl alcohol. The column packed with YWG C8 was used asanalytical column and 13% acetonitrile as mobile phase. Detector wavelength was set at 230nm.Th

Key words: Determination Identification HPLC Paeoniforin Fructus